摘要
在冰盐浴条件下,芳香族重氮盐与活泼亚甲基化合物反应,合成了六种新芳香族腙类衍生物.产物经IR,^(1)HNMR,^(13)CNMR,元素分析表征,其中3b和3e经X射线单晶衍射测定,确认了其化学结构.
Six kinds of phenyl hydrazones were synthesized by the reaction of ice bath using aromatic diazonium salt and active methylene compounds. The products were characterized via IR, ^1H NMR, ^13C NMR spectra and elemental analysis as well as single-crystal X-ray diffraction analysis of 3b and 3e.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2007年第4期524-527,共4页
Chinese Journal of Organic Chemistry
基金
洛阳师范学院重点学科(No.2004YZK90)资助项目.
关键词
腙
芳香族重氮盐
活泼亚甲基化合物
合成
hydrazone
aromatic diazonium salt
active methylene compound
synthesis
