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溶剂助蒸馏法在烟草香气成分分析中的应用 被引量:12

Application of Solvent Co-distillation in the Analysis of Tobacco Aroma Compounds
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摘要 通过溶剂助蒸馏法分离、收集烟草中的香气物质,用GC/MS进行了定性分析,并用内标法进行定量分析。对烟草中近30种主要香气物质进行了定量分析,探讨了分析方法的重复性,比较了溶剂助蒸馏与同时蒸馏萃取对分析结果的影响。溶剂助蒸馏方法简便、快速,易于操作,重复性令人满意,定量结果接近同时蒸馏萃取法。 Solvent co-distillation was employed to isolate and collect the aroma compounds of tobacco, which were then determined by GC/MS. The major aroma compounds in the isolated mixture were quantified with the internal standard (methyl nicotinate) added. Compared with the simultaneous distillation extraction (SDE), the solvent co-distillation was fast, convenient, and easy to operate. The ~atability was satisfactory. The obtained result was comparable to those obtained from SDE.
出处 《中国烟草科学》 CSCD 2007年第2期23-26,共4页 Chinese Tobacco Science
关键词 溶剂助蒸馏 GC/MS solvent co-distillation GC/MS
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  • 1常爱霞,贾兴华,郝廷亮,徐玉田,毕建立,厉昌坤,王允白.特香型烤烟挥发性致香物质的测定与分析[J].中国烟草科学,2002,23(1):1-5. 被引量:47
  • 2Kim Nam Sun,Lee Dong Sun.Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry.Journal of Chromatography A,2002,982:31-47.
  • 3Cai Jibao,Liu Baizhan,Su Qingde.Analysis of free and bound volatiles by gas chromatography and gas chromatography-mass spectrometry in uncased and cased tobaccos[J].Journal of Chromatography A.2002,947:267-275.
  • 4Misharina T A,Golovnya R V,Beletsky I V.Comparison of the efficiency of isolation of volatiles from foodstuffs by co-distillation and Likens-Nickerson methods//Maarse H.Heij D Van der.Developments in Food Sci.V35.Trends in Flavor Research,Elsevier,New York,1994,117.

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