摘要
目的:建立HPLC法测定三七止血胶囊中没食子酸含量的方法。方法:色谱柱为C18,以甲醇-0.05%磷酸溶液(15:85)为流动相,检测波长271nm。结果:平均回收率为99.3%,RSD为0.47%(n=5)。结论:该法简便、灵敏、准确,重现性好。
Objective:To establish an HPLC method for the determination of Gallic Acid in Sanqi Zhixue Capsule. Method:The HPLC method was developed for the determination of Gallic Acid in Sanqi Zhixue Capsule on C18 column, using methanol- 0. 05% phosphoric acid solution (15 : 85) as mobile phase ;detective wavelength at 271nm. Result:The average recovery is 99. 3 %and the RSD is 0. 47 % (n= 5). Conclusion:The method is simple,sensitive and accurate with good reproducibility.
出处
《中国药品标准》
CAS
2007年第2期70-72,共3页
Drug Standards of China