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毛细管气相色谱法测定多糖的单糖组成 被引量:7

Component analysis of monosaccharides composition in polysaccharide by capillary gas chromatography
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摘要 To analyze the monosaccharides composition and their molar ratio in Fuctus mume polysaccharide and Ligustrum japonica tea polysaccharide by using acetylation derivatization and capillary gas chromatography.The monosaccharides composition and their molar ratio of the Fuctus mume polysaccharide are: rhamnose:arabinose:xylose:mannose:glucose:galactose=0.65:4.96:0.93:1:7.03:8.61;the monosaccharides composition and their molar ratio of the Ligustrum japonica tea polysaccharide are: rhamnose:arabinose: xylose: mannose:glucose:galactose =1:3.31: 0.24:0.58:2.96:5.70.The method was established with the relative standard deviations and the recoveries being in the range of 0.37%~0.91% and 95.9 %~102.3 %,respectively. To analyze the monosaccharides composition and their molar ratio in Fuctus mume polysaccharide and Ligustrum japonica tea polysaccharide by using acetylation derivatization and capillary gas chromatography. The monosaccharides composition and their molar ratio of the Fuctus mume polysaccharide are : rhamnose: arabinose : xylose : mannose : glucose: galactose = 0. 65 : 4.96 : 0. 93 : 1:7.03:8.61 ;the monosaccharides composition and their molar ratio of the Ligustrum japonica tea polysaccharide are: rhamnose : arabinose : xylose : mannose: glucose: galactose = 1:3.31 : 0. 24:0.58:2.96:5.70. The method was established with the relative standard deviations and the recoveries being in the range of 0. 37%~0.91% and 95.9 % ~ 102.3 %, respectively.
出处 《化学研究与应用》 CAS CSCD 北大核心 2007年第5期521-523,共3页 Chemical Research and Application
关键词 乌梅多糖 苦丁茶多糖 单糖 毛细管气相色谱 Fuctus mume polysaccharide Ligustrum japonica tea polysaccharide monosaccharide capillary gas chromatography
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