摘要
The crystal structure of the title compound （C17H16N4O3S2, Mr = 388.46） has been determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P21/c with a = 13.688（2）, b = 16.704（3）, c = 8.3308（12）A, β = 99.474（6）°, V = 1878.8（5） A^3, Mr = 388.46, Z = 4, Dc = 1.373 g/cm3, μ = 0.308 mm^–1, F（000） = 808, R = 0.0389 and wR = 0.0917. X-ray analysis reveals that the crystal structure involves intermolecular N–H…O and N–H…N hydrogen bonds, which link the molecules into a layer parallel to the ac plane.
The crystal structure of the title compound （C17H16N4O3S2, Mr = 388.46） has been determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P21/c with a = 13.688（2）, b = 16.704（3）, c = 8.3308（12）A, β = 99.474（6）°, V = 1878.8（5） A^3, Mr = 388.46, Z = 4, Dc = 1.373 g/cm3, μ = 0.308 mm^–1, F（000） = 808, R = 0.0389 and wR = 0.0917. X-ray analysis reveals that the crystal structure involves intermolecular N–H…O and N–H…N hydrogen bonds, which link the molecules into a layer parallel to the ac plane.
基金
The project was supported by the National Natural Science Foundation of China (NSFC#20432010 and NSFC#20602021)
