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新鞣花酸衍生物的NMR归属(英文)

NMR Assignment of Two Ellagic Acid Derivatives
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摘要 从鞣花酸(1)合成二个新的多取代的联苯化合物3和4,利用HMQC, HMBC和一维NOE谱技术确定了它们的13C和1H NMR归属. Two polysubstituted biphenyl compounds were synthesized from ellagic acid. Using NMR techniques including HMQC, HMBC and 1D NOE techniques, the ^13C and ^1H NMR chemical shifts of the two product compounds were assigned.
作者 冀亚飞 张培成 于德泉
机构地区 华东理工大学制药工程系 中国医学科学院中国协和医科大学药物研究所
出处 《波谱学杂志》 CAS CSCD 北大核心 2007年第2期133-140,共8页 Chinese Journal of Magnetic Resonance
关键词 核磁共振 HMQC HMBC 一维NOE谱 联苯化合物 二异丁基氢化铝 NMR, HMQC, HMBC, 1D NOE, biphenyl compounds, Bu2 AIH
分类号 O641 [理学—物理化学]
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参考文献8

  • 1Do Khac D,Tran-Van S,Campos A M,et al.Ellagic compounds from diplopanax stachyanthus[J].Phytochemistry,1990,29(1):251-256.
  • 2Kadota S,Takamori Y,Khin N N,et al.Constituents of the leaves of wood fordia fruticosa Kurz.I.Isolation,structure,and proton and carbon-13 nuclear magnetic resonance signal assignments of woodfruticosin (woodfordin C),an inhibitor of deoxyrIbonucleic acid topoisomerase[J].Chem Pharm Bull,1990,38(10):2687-2 697.
  • 3Nawwar M A M,Marzouk M S,Nigge W,et al.High-performance liquid chromatographic/electrospray ionization mass spectrometric screening for polyphenolic compounds of epilobium hirsutum-The structure of the unique ellagitannin epilobamide-A[J].J Mass Spectrom,1997,32:645-654.
  • 4刘力军,缪振春,仲伯华,刘河,刘克良.一维NOESY和HOHAHA技术用于苯环壬酯的立体结构研究[J].波谱学杂志,2006,23(1):23-29. 被引量：5
  • 5Heur Y H,Zeng W,Stoner G D.Synthesis of ellagic acid O-alkyi derivatives and isolation of ellagic acid as a tetrahexanoyl derivative from fragaria ananassa[J].J Nat Prod,1992,55(10):1 402-1 407.
  • 6Li X C,Elsohly H N,Hufford C D,et al.NMR assignments of cllagic acid derivatives[J].Magn Reson Chem,1999,37:856-859.
  • 7Kashiwada Y,Huang L,Ballas L M,et al.New hexahydroxybiphenyl derivatives as inhibitors of protein kinase C[J].J Med Chem,1994,37(1):195-200.
  • 8张起辉,高慧媛,周莲娣,韩志超,吴立军.吴茱萸内酯的NMR研究(英文)[J].波谱学杂志,2005,22(1):1-5. 被引量：8

二级参考文献11

  • 1刘力军,仲伯华,缪振春.胸腺五肽的NMR研究[J].波谱学杂志,2005,22(2):201-207. 被引量：9
  • 2缪振春,罗毅,杜泽涵,冯锐.一种新的测定一维同核全相关的NMR技术[J].波谱学杂志,1996,13(1):11-17. 被引量：11
  • 3Anonymous.Encyclopedia of Chinese Medicine[M].Shanghai:Shanghai People's Press,1977.1 118.
  • 4Liu Yun-xiu,Luo Shu-rong.Progress in the research of Alkaloids in Evodia rutaecarpa[J].Nat Prod Res Dev,1998,12(1):87-93.
  • 5Sugimoto T,Miyase T,Kuroyanagi M,et al.Limonoids and quinolone alkaloids from Evodia rutaecarpa Bentham[J].Chem Pharm Bull,1988,36(11):4 453-4 461.
  • 6Liu Chuanhui,Yun Liuhong,Wen Guangling,et al.A composition for preventing and treating kinetotia syndrome [P].WO:95/11025,1994-10-22.
  • 7Liu Chuanhui,Liang Qishan,Gao Zhanguo,et al.Use of phencynonate hydrochloride [P].WO:02067933(A1),2004-08-05.
  • 8Arias-Perrez M S,Alejo A,Galvez E,et al.Structural study of ethyl-3-methyl-oxo-3 -azabicyclo [3,3,1] nonance-1- carboxylate by two - dimensional NMR spectroscopy [J].J Mol Struct,1995,349:169-174.
  • 9Iriepa I,Gil-Alberdi,Galvez E,et al.Structural,conformational and pharmacological study of some 3 - methyl-2,4 - diphenyl-3- azabicyclo [3,3,1] noman-9b-ol [J].J Mol Struct,1995,351:119-125.
  • 10相婷,吴立军,侯捷,周晓川.绿原酸乙酯的NMR研究(英文)[J].波谱学杂志,1997,14(5):387-391. 被引量：4

共引文献11

波谱学杂志
2007年 第2期

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