摘要
以1,4-萘醌为原料,经溴化、氰化、烷基化合成了1,4-二丙氧基-2,3-二氰基萘,用SiemensP4四圆衍射仪测得了晶体结构。合成方法简便,反应时间短,产率高。
1, 4 - Dipropoxynaphthalene-2, 3-dicarbonitriles was synthesized from 1,4-naphthoquinone by brodriation instead of chlorination, cyanation and alkylation. The Crys-tal stutalre of the titie compound was determined using siemens P4 four-cirde diffractometer.The modified method give the product at muth higher yields while using a simpler experimentalprocedure.
出处
《黑龙江大学自然科学学报》
CAS
1997年第1期95-97,共3页
Journal of Natural Science of Heilongjiang University
关键词
二丙氧基
二氧基萘
合成
晶体结构
1,4-dipropoxynaphthalene-2,3-dicarbonitriles
Synthesis, Crystal sturcture