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Cu(Ⅱ)与亚氨基二乙酸配合物的合成、晶体结构 被引量：2

Synthesis and Crystal Structure of [Cu(C_4H_5O_4N)(H_2O)_ 2]_ n
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摘要 存在2-氨基苯并噻唑时,利用高氯酸铜与亚氨基二乙酸反应,合成了一维链状配位聚合物[Cu(C4H5O4N)(H2O)2]n;通过X射线晶体衍射表征其晶体结构。 The reaction of Cu （ClO4 ）2 · 6H2O with iminodiacetic acid in 50% ethanol solution containing 2- Aminobenzolthiazole, forms [ Cu （ C4H5O4N） （H2O）2 ] n complex is presented. Single crystal X-ray diffraction analysis shows that its structure was one-dimensional polymerical chain
作者 郑典慧 陈定奔 黄凌
机构地区 浙江工业大学化材学院 台州学院医药化工学院
出处 《科学技术与工程》 2007年第12期2940-2942,共3页 Science Technology and Engineering
关键词 铜 聚合物 晶体结构 copper polymer crystal structure
分类号 O723.2 [理学—晶体学]
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参考文献2

  • 1[1]Wang J,Song X M,Zhang W Q,et al.Investigation on molecular and crystal structures of metal complexes with aminopolycarboxylic acids(Ⅰ) -synthesis and structure of Na2[FeⅢ(ida)2]2·3H2O.Chinese Chemical letters,1997; 8(8):48-51
  • 2[4]Román-Alpiste M J,Martín-Ramos J D,Castifieeiras-Campos A,et al.Synthesis,XRD structures and properties of diaqua(iminodiacetato) copper(Ⅱ),[Cu (IDA) (H2 O) 2],and aqua (benzimidazole)(iminodiacetato) copper(Ⅱ),[Cu (IDA) (HBzIm) (H2O)].Polyhedron,1999; 18:571-577

同被引文献31

  • 1Roman-Alpiste M J, Martin-Ramos J D, Castifieiras-Campos A, et al. Synthesis, XRD structures and properties of diaqua (iminodiacetato) copper(II), [Cu(IDA)(H2O)2], and aqua (benzimidazole) (iminodiacetato)copper(II), [Cu(IDA)(HBzlm)(H2O)]. Polyhedron, 1999, 18(25): 3341-3351.
  • 2Hu C C, Chen W C, Chang K H. How to achieve maximum utilization of hydrous ruthenium oxide for supercapacitors. J. Electrochem. Soc., 2004, 151(2): A281-A290.
  • 3Liu K C, Anderson M A. Porous nickel oxide/nickel films for electrochemical capacitors. J. Electrochem. Soc., 1996, 143(1): 124-130.
  • 4Nam K W, Kim K B. A study of the preparation of NiOx electrode via electrochemical route for supercapacitor applications and their charge storage mechanism. J. Electrochem. Soc., 2002, 149(3): A346-A354.
  • 5Yu C C, Zhang L X, Shi J L, et al, A simple template-free strategy to synthesize nanoporous manganese and nickel oxides with narrow pore size distribution, and their electrochemical properties. Adv.Funct.Mater., 2008, 18(10): 1544-1554.
  • 6Yuan C Z, Zhang X G, Su L H, et al. Facile synthesis and self-assembly of hierarchical porous NiO nano/micro spherical superstructures for high performance supercapacitors. J. Mater. Chem., 2009, 19(32): 5772-5777.
  • 7Wu M S, Huang Y A, Yang C H. Capacitive behavior of porous nickel oxide/hydroxide electrodes with interconnected nanoflakes synthesized by anodic electrodeposition. J. Electrochem. Soc., 2008, 155(11): A798-A805.
  • 8Nam K W, Kim K H, Lee E S, et al. Pseudocapacitive properties of electrochemically prepared nickel oxides on 3-dimensional carbon nanotube film substrates. J.Power Sources, 2008, 182(2): 642-652.
  • 9Nathan T, Aziz A, Noor A F, et al. Nanostructured NiO for electrochemical capacitors: synthesis and electrochemical properties. J. Solid State Electrochem., 2008, 12(7): 1003-1009.
  • 10Cheng J, Cao G P, Yang Y S. Characterization of Sol-Gel-derived NiOx xerogels as supercapacitors. J. Power Sources, 2006, 159(1): 734-741.

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科学技术与工程
2007年 第12期

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