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石英微量天平/热传导量热仪

Quart Crystal Microbalance/Heat Conduction Calorimetry
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摘要 石英微量天平是一种新型高效的薄膜热分析和热量测定仪器。薄膜的物理和化学性质均可以在此仪器上得到研究。水的吸附,药物薄膜的软化行为,富勒稀碳分子膜中溶剂的提取是其典型的应用。也可用于油漆和喷釉的烘干和加工以及通过监控质量的变化和新陈代谢的放热进行营养环境中生长细菌的检测。 The quartz crystal microbalance is a powerful new instrument concept in the area of thermal analysis and calorimetry of thin films. Both the physical and chemical properties of films can be investigated. Typical applications are water uptake and softening of pharmaceutical film coats, solvent uptake in fullerene films, drying and curing of paints and spray-on enamel, and detection in the early stages of bacterial growth on a nutrient medium by monitoring mass change and metabolic heat evolution.
作者 AllanL.Smith
机构地区 Masscal Corp.
出处 《生命科学仪器》 2007年第5期28-32,共5页 Life Science Instruments
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参考文献14

  • 1[1]Smith AL,Shirazi H,Wadso I.The QCM/HCC:simultaneous,isothermal,high sensitivity measurements of mass change and heat flow in polymer and fullerene films.In:Ruoff RS,Kadish KD,eds.Recent advances in the chemistry and physics of fullerenes and related materials.vol.98-8:576-85.San Diego,CA:Electrochemical Society,1998.
  • 2[2]Smith AL.Shirazi HM.Quartz microbalance microcalorimetry:a new method for studying polymer-solvent thermodynamics.J Therm Anal Calorim 2000;59:171-86.
  • 3[3]Smith AL,Mulligan SR,Tian J,Shirazi H,Riggs JC.A mass/heat flow sensor combining shear mode resonators with thermoelectries:principles and applications.Presented at IEEE Frequency Control Symposium,Tampa,FL,May 2003.
  • 4[4]Smith AL.Mass and heat flow measurement sensor.2000.U.S.patent no.6,106,149.
  • 5[5]Buttry DA.Ward MD.Measurement of interfacial processes at electrode surfaces with the electrochemical quartz crystal microbalance.Chem Rev 1992;92:1355-79.
  • 6[6]Smith AL.Mulligan SR,Shirazi HM.Determining the effects of vapor sorption in polymers using the quartz crystal microbalance/heat conduction calorimeter.J Polym Sci Part B Polym Phys 2004;42:3893-3906.
  • 7[7]Smith AL.Rheological measurements in thin films plasticized by solvents:an application of the quartz crystal microbalance.J Polym Sci Part B Polym Phys 2004,in press.
  • 8[8]Smith AL.Zilberman G.Detection of vital bacteria and protein ligand binding using the QCM/HCC.In:Rich M,ed.2004 NATAS.Williamsburg,VA:NATAS,2004.
  • 9[9]Tian J.Applications of quartz crystal microbalance/heat conduction calorimetry.Ph.D.thesis,Drexel University,Philadelphia,PA,2003.
  • 10[10]Shirazi HM.Quartz crystal microbalance/heat conduction calorimetry(QCM/HCC),a new technology capable of isothermal,high sensitivity,mass and heat flow measurements at a solid/gas interface.Ph.D.thesis,Drexel University,Philadelphia,PA,2000.

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