常用软坚散结中药及复方碘含量的测定

To Mensurate the Content of Iodine in Herbal Medicine and Compound Prescription Used in Softening Hard Mass and Disintegrating Masses

目的:测定常用软坚散结中药及复方的碘含量。方法:从大量古今文献中筛选常用于治疗瘿病的软坚散结中药及复方,碱灰化法消化固体饮片,常规水煎中药及复方煎剂,采用中华人民共和国卫生部行业标准规定的方法:砷铈催化分光光度法。同一标本连续测定3次,取平均值。结果:海藻饮片碘含量682.46μg/kg,煎剂碘含量1951.75μg/L;昆布饮片碘含量794.69μg/kg,煎剂碘含量1760.85μg/L;黄药子饮片碘含量4.69μg/kg,煎剂碘含量54.24μg/L;海藻玉壶汤碘含量1951.75μg/L;除去海藻、昆布、海带的海藻玉壶汤碘含量51.39μg/L;消瘿瘤汤碘含量3829.50μg/L。结论:海藻、昆布为碘含量丰富的中药即富碘中药,海藻玉壶汤、消瘿瘤汤为富碘复方。

Objective ：To mensurate the content of iodine in herbal medicine and compound prescription used in softening hard mass and disintegrating masses. Methods ：selected herbal medicine and compound prescription from masses of literature in all times,which were used in curing goiter,digestion fixed the herb of small pieces ALkali-ash method,decoeted herbal medicine and eompulnd prescription routinely, using People＇s Republic of China medicaldepartment profession standard stipulation：Arsenieeerium catalysis spectrophotometrie method. The same sample was mensurated three times ,we chose the average. Results ：the content of iodine in algae （hearb of small pieces） was 682. 46μg/kg,while the result in decoction was 1951.75μg/L;the content of iodine in duubu （herb of small pieces） was 794.69μg/kg,while the result in decoction was 1760.85μg/L;the content of iodine in huangyaozi （herb of small pieces） was 4.69μg/kg,while the result in decoction was 54.24μg/L; the content of iodine in the 51.39 μg,/L with the exception of algae, kubu, haidai ; the content of iodine in the decoction of xiaoyingliu was 3829.50μg/kg. Conclusion ： Algae and Kubu were full of iodine in herbal modieine, as well as the decoction of haizaoyuhu and the decoction of xiaoyingliu in compound prescription.