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对甲基苯磺酸催化合成巯基化壳聚糖研究 被引量：1

Synthesis of Chitosan-Thiolated Polymers Catalyzed by P-Toluenesulfonic Acid
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摘要 以对甲基苯磺酸为催化剂,巯基乙酸和壳聚糖为原料合成了巯基化壳聚糖.在壳聚糖和巯基乙酸比例(W/V)为0.05,催化剂0.08g、反应时间24h、温度为25℃的反应条件下,巯基含量达到6.10%. Chitosan-thiolated polymers was synthesized by mercaptoacetic acid and chitosan catalyzed by p-toluenesulfonic acid. The results show that the appropriate conditions are： ratio of chitosan to mercaptoacetic acid is 0.05（W/V）, weight of catalyst is 0.08g, reaction time is 24h, temperature is 25℃, Under the appropriate conditions the yield of the high-density thiol groups was 6.10%.
作者 王瑞霞 卢基林 张玉军
机构地区 河南工业大学化学化工学院 湖南文理学院化学化工系
出处 《襄樊学院学报》 2007年第5期45-47,共3页 Journal of Xiangfan University
基金 河南省教育厅自然科学基金项目(2004150010) 河南工业大学基金项目(0400012)
关键词 壳聚糖 催化 巯基化 Chitosan Catalysis Thiolated polymers
分类号 O62 [理学—有机化学]
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参考文献8

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二级参考文献2

共引文献9

同被引文献13

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襄樊学院学报
2007年 第5期

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