期刊文献+

An improved procedure for the synthesis of 4-methylimidazol-2-one

An improved procedure for the synthesis of 4-methylimidazol-2-one
下载PDF
导出
摘要 A novel one-pot synthetic method of 4-methylimidazol-2-one is described. The target compound is conveniently synthesized from sodium diformylamide, a modified Gabriel reagent prepared, through condensation, hydrolyzation and cyclization reactions without separating intermediates, its total yield is 75.8%.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2007年第7期777-778,共2页 中国化学快报(英文版)
关键词 4-Methylimidazol-2-one SYNTHESIS Sodium diformylamide 4-Methylimidazol-2-one Synthesis Sodium diformylamide
  • 相关文献

参考文献7

  • 1[1]R.Duschinsky,L.A.Dolan,J.Am.Chem.Soc.67 (1945) 2079.
  • 2[2]R.A.Schnettler,R.C.Dage,J.Med.Chem.25 (12) (1982) 1477.
  • 3[3]P.Cui,T.L.Macdonald,M.Chen,et al.Bioorg.Med.Chem.Lett.16 (13) (2006) 3401.
  • 4[4]Y.H.Chen,C.S.Sun,Y.C.Rui,Acta Pharm.Sin.23 (1) (1988) 21 (in Chinese).
  • 5[5]S.T.Ma,Chin.J.Pharm.30 (12) (1999) 529 (in Chinese).
  • 6[6]Y.H.Liu,G.Sun,A.David,et al.Chem.Res.Toxicol.17 (1) (2004) 110.
  • 7[7]Y.L.Han,H.W.Hu,Synthesis 7 (1990) 122.

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部