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Al_2O_3粉末对镁合金微弧氧化陶瓷膜的显微结构及其耐蚀性的影响 被引量:15

INFLUENCE OF ADDITIONS OF Al_2O_3 POWDERS IN ELECTROLYTICAL SOLUTION ON MICROSTRUCTURE AND CORROSION PROTECTION OF CERAMIC COATINGS FORMED ON MAGNESIUM ALLOY DURING MICRO-ARC OXIDATION
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摘要 在已优化的Na2SiO4-Na3PO4复合体系溶液中加入Al2O3粉末对AZ91D镁合金进行了微弧氧化处理。用SEM、XRD分析了加入Al2O3粉末对陶瓷膜的形貌特征和相成分的影响。结果表明,加入Al2O3粉末后陶瓷膜孔洞减少,且疏松层变得紧实;膜层相成分增加了Al2O3。在3.5%NaCl溶液中的电化学腐蚀试验表明,加入Al2O3粉末后陶瓷膜的耐蚀性有很大提高。 AZ91D magnesium alloy was treated by micro-arc oxidation (MAO) in the optimized composite solution of silicate-phosphate system in which Al2O3 powders were added.Morphological characteristic and phase constituent of ceramic coatings were analyzed using the scanning electron microscope (SEM) and the x-ray diffraction (XRD).The results showed that after adding Al2O3 powders pores in ceramic coatings decreased and the loose layer became more compact,new phase of Al2O3 appeared.Electrochemical corrosion experiments in 3.5% NaCl solution showed that corrosion resistance of ceramic coatings after adding Al2O3 powders was also improved greatly.
出处 《中国腐蚀与防护学报》 CAS CSCD 北大核心 2007年第4期202-205,共4页 Journal of Chinese Society For Corrosion and Protection
基金 山西省教委科技开发项目(20041214) 山西省自然基金(20041065)
关键词 镁合金 Al2O3粉末 微弧氧化 形貌特征 相成分 耐蚀性 magnesium alloy,Al2O3 powders,micro-arc oxidation,morphological characteristic,phase constitution, corrosion resistance
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