摘要
报道了一种简单有效的合成N-取代乙酰胺的新方法.在微波辐射、无溶剂条件下,1.5摩尔比率的乙酸酐和一系列胺发生反应合成15个N-取代乙酰胺,该方法操作简便,反应时间短,产率高.更重要的是该方法适用范围较广(脂肪胺、芳香胺、杂环胺).环境友好.
In this paper, a facile and efficient method was developed for preparing N-substituted acetamides under microwave irradiation. The reaction time is short and the yields are high. What is more, the protocol considerably broadens the scope of amines compared with the microwave-assisted synthesis of amides directly from carboxylic acid.
出处
《河南师范大学学报（自然科学版）》
CAS
CSCD
北大核心
2007年第3期88-90,共3页
Journal of Henan Normal University(Natural Science Edition)
基金
中国科学院知识创新工程重要方向项目(KGCX2-SW-602-5)
关键词
微波
无溶剂
N-取代乙酰胺
合成类型
microwave irradiation
solvent-free
N-substltuted acetamides
synthesis
