电解合成卤仿的研究——简易电极材料电解氧化合成碘仿(Ⅱ)

A Synthetic Method of Iodoform by Electrolytic Oxidation in Some Electrode Materials (Ⅰ)

本文报道采用镍(Ni)、铅(Pb)、过氧化铅(PbO_2)等材料作为工作电极,在简易电解槽中进行电解氧化合成碘仿(CHI_3)。在不使用电解隔膜的条件下,产率为65—74％。

This paper reports a synthetic mathod of iodoform by electrolytic oxidation in the simply equipped electrolytic bath, in which nickel, lead and lead dioxide were used as working electrodes, the result is good.