摘要
目的建立健胃消炎颗粒有效成分含量测定方法,控制健胃消炎颗粒的产品质量,确保其临床疗效。方法采用高效液相色谱法对健胃消炎颗粒中白芍、赤芍的有效成分芍药苷含量进行了测定,并进行了方法学研究;同时应用薄层色谱法对其君药党参进行定性鉴别。结果芍药苷进样量在0.1086～0.5430μg之间有良好线性,回收率理想。结论薄层色谱法对样品分离效果好。
Objective To control the quality of Jianwei Xiaoyan Keli and ensure its effect in clinical application. Methods Using phase liquid chromatography,the active component of paeoniflorin in radix paeoniae alba and radix paeoniae rubra of this medicine was determined,and radix codonopsis used as primary constituent of Jianwei Xiaoyan Keli was detected using TLC scanning method. Results The sample size of paeoniflorin at 0.108 6～0.543 0 μg showed good linearity with ideal recovery rate. Conclusion Thin-layer chromatography is good for sample separation.
出处
《齐鲁医学杂志》
2007年第5期447-448,450,共3页
Medical Journal of Qilu
关键词
健胃消炎颗粒
薄层鉴别
高效液相色谱
芍药苷
Jianwei Xiaoyan Keli
thin-layer chromatography
phase liquid chromatography
paeoniflorin
