期刊文献+

Synthesis and application of an IL-supported diol as protecting group for aldehydes 被引量:1

Synthesis and application of an IL-supported diol as protecting group for aldehydes
下载PDF
导出
摘要 新支持 IL 的 diol, 1-(2,3-dihydroxypropyl )-3-methylimidazolium hexafluorophosphate 被英尺红外, 1H NMR, 13C NMR 和 MS (ESI ) 综合了并且描绘。它象冻结点,溶解度和比重和热稳定性那样的物理性质是坚定的。为醛的一个保护的组也被调查的结果的 diol 的合成实用程序。 A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by Fr-IR, ^1H NMR, ^13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic utilities of the resultant diol as a protecting group for aldehydes were also investigated.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2007年第10期1205-1208,共4页 中国化学快报(英文版)
基金 the National Natural Science Foundation of China(No.20533010,20673039) the Science&Technology Commission of Shanghai Municipality(No.06JC14023)for financial support.
关键词 二醇 保护作用 化学 IL-supported diol Preparation Characterization Protecting group
  • 相关文献

参考文献9

  • 1[1]For reviews,see:(a) T.Welton,Chem.Rev.99 (1999) 2071;(b)K.R.Seddon,J.Chem.Technol.Biotechnol.68 (1997) 351;(c)P.Wasserscheid,W.Keim,Angew.Chem.Int.Ed.39 (2000) 3772;(d) K.R.Seddon,A.Stark,M.J.Torres,Pure Appl.Chem.72 (2000) 2275;(e)R.Sheldon,Chem.Commun.(2001) 2399;(f)J.Dupont,R.F.de Souza,P.A.Z.Suarez,Chem.Rev.102 (2002) 3667.
  • 2[2]J.H.Davis Jr.,Chem.Lett.33 (2004) 1072.
  • 3[3](a) J.Fraga-Dubreuil,J.P.Bazureau,Tetrahedron Lett.42 (2001) 6097;(b)W.Miao,T.H.Chan,Org.Lett.5 (2003) 5003;(c)F.Yi,Y.Peng,G.Song,Tetrahedron Lett.46 (2005) 3931;(d)M.de Kort,A.W.Tuin,S.Kuiper,H.S.Overkleeft,G.A.V.Marel,R.C.Buijsman,Tetrahedron Lett.45 (2004) 2171.
  • 4[4]G.H.Song,Y.Q.Cai,Y.Q.Peng,J.Comb.Chem.7 (2005) 561.
  • 5[5](a) J.H.Davis Jr.,K.J.Forrester,Tetrahedron Left.40 (1999) 1621;(o) D.M.Li,F.Shi,J.J.Peng,S.Guo,Y.Q.Deng,J.Org.Chem.69 (2004) 3582;(c) D.M.Li,F.Shi,S.Guo,Y.Q.Deng,Tetrahedron Lett.4 (2004) 265.
  • 6[6](a) J.H.Davis Jr.,K.J.T.Forrester,J.Merrigan,Tetrahedron Lett.49 (1998) 8955;(b) T.J.Merrigan,E.D.Bates,S.C.Dorman,J.H.Davis Jr.,Chem.Commun.(2000) 2051;(c) E.Visser,R.P.Swatloski,W.M.Reichert,Chem.Commun.(2001) 135;(d) F.Favre,H.O.Bourbigou,D.Commereuc,L.Saussine,Chem.Commun.(2001) 1360;(e)P.Wasserscheid,B.D.H(o)lscher,Chem.Commun.(2003) 2038;(f)J.J.Jodry,K.Mikami,Tetrahedron Lett.45 (2004) 4424;(g)E.D.Bates,R.D.Mayton,I.Ntai,J.H.Davis,J.Am.Chem.Soc.124 (2002) 926.
  • 7[7](a) T.W.Reene,P.G.M.Wuts (Eds.),Protective Groups in Organic Synthesis,John Wiley and Sons,New York,1999;(b)J.R.Hanson (Ed.),Protecting Groups in Organic Synthesis,Blackwell Science,Inc.,Malden,MA,1999;(c)P.J.Kocienski (Ed.),Protecting Groups,Georg Thieme Verlag,Stuttgart,1994.
  • 8[8](a) C.C.Leznoff,J.Y.Wong,Can.J.Chem.51 (1973) 3756;(b)C.C.Leznoff,S.Greenberg,Can.J.Chem.54 (1976) 3824;(c)C.C.Leznoff,W.Sywanyk,J.Org.Chem.42 (1977) 3203;(d)J.M.J.Fréchet,E.Bald,F.Svec,Reactive Polym.1 (1982) 21;(e)P.Hodge,J.Waterhouse,J.Chem.Soc.,Perkin Trans.I (1983) 2319.
  • 9[9]J.G.Huddleston,A.E.Visser,W.M.Reichert,H.D.Willauer,G.A.Broker,R.D.Rogers,Green Chem.3 (2001) 156.

同被引文献2

引证文献1

二级引证文献6

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部