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介孔分子筛MCM-41的合成探索 被引量:1

Explore in Synthesis of Mesoporous Materials MCM-41
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摘要 以正硅酸乙酯(TEOS)为硅源、十六烷基三甲基溴化铵(CTAB)为模板剂,利用水热合成法制备了介孔氧化硅MCM-41,并采用TEM、XRD、N2吸附-脱附等测试手段对产物进行了表征。结果表明,合成的介孔材料为高质量的MCM-41。 By using tetraethyl ortho-silicate(TEOS) as silica source, cetyltrimethyl ammonium bromide(CTAB) as the template,the mesoporous silica materials were synthesized by hydrothermal synthesis, the structure was investigated by means of TEM, XRD, Nz adsorption- desorption isotherms. The characteristic results showed that the MCM-41 mesoporous material had high quality.
作者 张丹 张英菊
出处 《山东陶瓷》 CAS 2007年第5期3-6,共4页 Shandong Ceramics
关键词 介孔材料 MCM-41 水热合成 等温吸附 Mesoporous Material MCM- 41 hydrothermal Synthesis Isothermal Adsorption
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参考文献13

  • 1Beck J S,Vartuli J C,Roth W J,et al. A new family of mesoporous molecular sieves prepared with liquid crystal templates. J Am Chem Soc,1992,114:10834-10843
  • 2Kresge C T, Leonowica M E, Roth W J,et al. Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism. Nature, 1992,359:710-712
  • 3王连洲,施剑林,禹剑,严东生.介孔氧化硅材料的研究进展[J].无机材料学报,1999,14(3):333-342. 被引量:41
  • 4王旭华,钱家盛,章于川.有序二氧化硅介孔固体材料制备的研究进展[J].过程工程学报,2004,4(1):84-89. 被引量:4
  • 5Gu G,Ong P P,Chu C. Thermal stability of mesoporous siliea moleeular sieves. J Phys Chem Solid, 1999,60: 943-947
  • 6丁彩凤,朱海涛,王海亭.表面活性剂在有序介孔材料合成中的应用[J].山东陶瓷,2003,26(3):10-14. 被引量:9
  • 7Whitehurst D D. Method to remove organic templates from freshly synthesized molecular sieves. U S Patent5, 1992, 143:879
  • 8Subramaniam B, Lyon CJ, Arunajatesan V. Environmentally benign multiphase catalysis with dense phase carbon dioxide. Appal Catal B: Environ, 2002,37 .. 279- 292.
  • 9周春晖,张波,李庆伟,蔡晔,葛忠华.反应介质对MCM-41介孔分子筛合成的影响研究[J].浙江工业大学学报,2001,29(2):110-114. 被引量:9
  • 10Lin W Y, Cai Q, Pang W Q, et al. New Mineralization Agents for the Synthesis of MCM-41 [J]. Microporous Mesoporous Mater, 1999,33 : 187- 196

二级参考文献84

  • 1王连洲 施剑林 等.-[J].无机材料学报,1998,14(1).
  • 2何家跃 鲍书林 等.-[J].科学通报,1997,2:66-168.
  • 3王连洲 禹剑 等.-[J].硅酸盐学报,.
  • 4陈逢喜 陈海鹰 颜学武 等.混合阴阳离子表面活性剂为膜板剂合成MCM-48型中孔分子筛[P].中国专利.CN1188689A.(1998).
  • 5何农跃,鲍书林,须沁华.含La的SiMCM-41的合成及其水热稳定性[J].科学通报,1997,42(2):166-168. 被引量:3
  • 6K.S.W. Sing, D.H. Everett, K.H.W. Haul, L.Moscou, R.A.Pierotti, J.Rouguerol, Pure Appl. Chem. 1985.57.603.
  • 7C.T. Kresge. M.E. Leonowiez, W.J. Roth, J.C. Vamdi, J.S.Beck, Nature 1992,359,710.
  • 8Yang. P, Zhao D, Margolese DI, et al. Genendized synthesis of large- pore mesoporous metal oxides with semicrystalline fraraeworks. Nature, 1998, 396: 152- 155.
  • 9Maclachan MJ. CoombsN, Ozin G A, Non - aqueous supramolecular assembly of mesostmctred metal gemmnimn sulphides from(Ge4S10)^4- clusters. Nature, 1999,397:681 - 684.
  • 10Q. Huo, D. I. Margolese , U. Ciesla, R. Leon, G.D.Study,Chem. Mater. 1994,6,1176 - 1191.

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