摘要
通过顺丁烯二酸酐水解并与双环戊二烯发生酸催化加成反应,合成了标题化合物(DHCM),收率达90%,产品中w(DHCM)>85%。通过元素分析、红外光谱和GC-MS等对其结构进行了表征。
Dicyclopentadiene monomaleate(DHCM),a new functional monomer,was prepared by hydrolysis of maleic anhydride(MA) followed by acid-catalyzed addition reaction with dicyclopentadiene(DCPD),and the yield of DHCM was up to 90% with its purity exceeding 85%.The molecular structure of product was characterized by EA,FT-IR spectroscopy and GC-MS,and the synthetic technology and performance of DHCM were also studied.
出处
《化学试剂》
CAS
CSCD
北大核心
2007年第11期667-669,共3页
Chemical Reagents