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微波辐射下8-取代嘌呤核苷的绿色合成 被引量：1

Green Synthesis of 8-Substituted Purine Nucleosides under Microwave Irradiation
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摘要 8-溴嘌呤核苷与亲核试剂在水溶液中,于400W,95℃微波辐射5min合成了10种8-取代嘌呤核苷,收率72%～92%,其结构经1HNMR和13CNMR表征。 8-Substituted purine nucleosides in yield of 72% - 92% were synthesized from 8-bromopurine nucleoside and nucleophilic reagent at 95 ℃ and 400 W under microwave irradiation for 5 min in water. The structures were characterized by ^1H NMR and ^13C NMR.
作者 渠桂荣 夏然 杨西宁 王东超
机构地区 河南师范大学化学与环境科学学院
出处 《合成化学》 CAS CSCD 2007年第6期756-758,762,共4页 Chinese Journal of Synthetic Chemistry
基金 国家自然科学基金资助项目(20772024)
关键词 8-取代嘌呤 微波辐射 绿色合成 8-substituted purine microwave irradiation green synthesis
分类号 R914.5 [医药卫生—药物化学] O621.25 [理学—有机化学]
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参考文献9

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共引文献8

同被引文献14

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引证文献1

合成化学
2007年 第6期

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