合成3,3′-二吲哚基苯基甲烷的新方法

A New Method for the Synthesis of 3,3′-Di-indoly-phenylmethane

以无水乙醚为溶剂,室温下无水三氯化铝催化N-(2-氯乙基)苯甲醛亚胺与吲哚反应,合成了3,3′-二吲哚基苯基甲烷和6,12-二苯基吲哚[2,3-b]咔唑,其结构经1HNMR,IR和MS表征。

3,3′-Di-indoly-phenylmethane and 6,12-di-phenyl-indolo [ 2,3-b ] carbazole were synthesized by the reaction of N-（2-chloroethyl） benzaldimines and indole in the presence of aluminium trichloride at room temperature. Their structures were characterized by ^1H NMR, IR and MS.