期刊文献+

铋膜电极伏安法测定苏丹红Ⅰ号 被引量:3

Determination of sudanⅠusing bismuth-film electrode by voltammetry
下载PDF
导出
摘要 The electrochemical of sudanⅠat an bismuth-film electrode has been studied.In the buffer solution of HAc-NaAc and ethanol(pH = 4.0),sudanⅠproduces an reductive peak at-0.5V,peak current showed a well linear relationship with concentration of sudanⅠin the range of 1.7×10-6mol/L~5.9×10-5mol/L,and to regression equation to ip =4.862+ 7.374C(×10-6mol/L),r=0.9978。 The limit of the detection is 8.1×10-7mol/L.This method can be applied to detemine sudanⅠ. The electrochemical of sudan Ⅰ at an bismuth - film electrode has been studied. In the buffer solution of HAc - NaAc and ethanol(pH = 4.0) ,sudan Ⅰ produces an reductive peak at -0.5V,peak current showed a well linear relationship with concentration of sudan Ⅰ in the range of 1.7× 10^-6mol/L -5.9 × 10^-5mol/L,and to regression equation to ip =4. 862 + 7. 374C( × 10^-6 tool/L) ,r =0. 9978, The limit of the detection is 8.1 × 10^-7mol/L. This method can be applied to detemine sudan Ⅰ.
作者 杜美菊
出处 《化学研究与应用》 CAS CSCD 北大核心 2007年第7期838-840,共3页 Chemical Research and Application
基金 河南省自然科学基金项目(0511020300)
关键词 苏丹红Ⅰ号 铋膜电极 循环伏安法 差分脉冲伏安法 sudan Ⅰ bismuth - film electrode cyclic voltammetry differential pulse vohammetry
  • 相关文献

参考文献6

二级参考文献11

  • 1张裕平,张毅军,袁倬斌,吴奇.高效液相色谱法测定红辣椒制品中的苏丹红[J].生命科学仪器,2005,3(3):25-28. 被引量:18
  • 2喻凌寒,杨运云,闫世平,陈江韩,李光宪,牟德海,蔡大川.LC—ESI/MS分析食品中微量苏丹红Ⅰ~Ⅳ[J].分析测试学报,2005,24(4):28-31. 被引量:46
  • 3梁景波,黄锦燕.反相高效液相色谱法检测辣椒酱中的苏丹红染料[J].化学分析计量,2005,14(5):27-29. 被引量:9
  • 4甘源,赵舰,肖义夫,王正虹,顾万江.反相高效液相色谱法测定食品中的苏丹红1号[J].现代预防医学,2005,32(12):1760-1761. 被引量:6
  • 5[1]PIELESZ A, BARANOWSKA I, RYBAKT A, et al. Detection and determination of a romatic amines as products of reductive splitting from selected azo dyes [J ] .Ecotoxicol Environ Saf.2002, 53: 42~47
  • 6[2]NAGASE M, OSAKI Y, MATSUEDA T.Determination of methyl yellow, Sudan I and Sudan II in water by high-performance liquid chromatography[J].J Chromatogr .1989 , 465: 434~437
  • 7[3]CALBIANI F, CARERI M, ELVIRI L, et al.Development and in-house validation of a liquid chromatographyC electrosprayC tandem mass spectrometry method for the simultaneous determination of Sudan I, Sudan II, Sudan III and Sudan IV in hot chilli products [J ].Journal of Chromatography A, 2004, 1042: 123~130
  • 8GB/T19681-2005.食品中苏丹红染料的检测方法-高效液相色谱法[S].[S].国家质量监督检验检疫总局,国家标准化管理委员会,2005..
  • 9.苏丹红危险性评估报告[R].北京:中华人民共和国卫生部,2005..
  • 10.欧盟危害物质新方法声明:03/99[Z].,..

共引文献69

同被引文献54

引证文献3

二级引证文献27

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部