摘要
通过文献方法合成了二茂铁乙炔及4-碘代-4′-硝基联苯,然后在PdCl2(PPh3)2/CuI催化作用下进行C-C偶联反应,得到新化合物4-二茂铁乙炔基-4′-硝基联苯.利用元素分析,IR,UV-Vis,MS等方法对新化合物进行了表征,并推测了新化合物的组成和结构.
A new compound 4-ferroceneacetenyl-4＇-nitrobiphenyl was synthesized by the reaction of ferroceneacetylene and 4＇-iodo-4＇-nitrobiphenyl,with PdCl2（PPh3）2 and CuI used as catalysts. The new compound was characterized by means of IR,UV-Vis,MS and elemental analysis. Its component and structure are given.
出处
《内蒙古工业大学学报（自然科学版）》
2007年第3期206-209,共4页
Journal of Inner Mongolia University of Technology：Natural Science Edition
基金
博士学科点专项科研基金(20060128001)
内蒙古自然科学基金
