摘要
以固体K2CO3为载体,在微波辐射无溶剂条件下,脱氧胆酸甲酯与芳酰氯反应合成了9个新的脱氧胆酸裂口分子人工受体,其结构经1HNMR,IR,MS及元素分析表征。
Nine new molecular clefts based on deoxycholic acid were synthesized by the reaction of methyl deoxycholate with aroyl chloride using solid K2CO3 as a supporter in solvent-free under microwave irradiation. The structures were characterized by ^1H NMR, IR, MS and elemental analysis.
出处
《合成化学》
CAS
CSCD
2008年第1期28-32,共5页
Chinese Journal of Synthetic Chemistry
关键词
脱氧胆酸
裂口分子
微波合成
分子识别
deoxycholic acid
molecular clefts
microwave synthesis
molecular recognition
