摘要
N-[1-（2-Methyl-1-methylcarbamoyl-propylcarbamoyl）-2,3-diphenyl-cyclopropyl]-ben- zamide, C29H31N3O3, has been synthesized and characterized by IR, ^1H NMR, ^13C NMR and singlecrystal X-ray diffraction. The crystal is of orthorhombic, space group P212121 with a = 11.0855（11）, b = 18.7756（19）, c = 24.434（2）A, V = 5085.5（9）A^3, Z = 8, Mr = 469.57, Dc = 1.227 g/cm^3, λ = 0.71070 A,μ（MoKα） = 0.080 mm^-1, F（000） = 2000, the final R = 0.0579 and wR = 0.1111 for 4569 observed reflections with I 〉 2σ（I）. The N-H and oxygen atom are involved in intermolecular hydrogen bonds which link the molecules into a one-dimensional chain.
N-[1-（2-Methyl-1-methylcarbamoyl-propylcarbamoyl）-2,3-diphenyl-cyclopropyl]-ben- zamide, C29H31N3O3, has been synthesized and characterized by IR, ^1H NMR, ^13C NMR and singlecrystal X-ray diffraction. The crystal is of orthorhombic, space group P212121 with a = 11.0855（11）, b = 18.7756（19）, c = 24.434（2）A, V = 5085.5（9）A^3, Z = 8, Mr = 469.57, Dc = 1.227 g/cm^3, λ = 0.71070 A,μ（MoKα） = 0.080 mm^-1, F（000） = 2000, the final R = 0.0579 and wR = 0.1111 for 4569 observed reflections with I 〉 2σ（I）. The N-H and oxygen atom are involved in intermolecular hydrogen bonds which link the molecules into a one-dimensional chain.
基金
the Foundation of 100 Young and Middle-aged Disciplinary Leaders of Guangxi Province in the 21st century (No. 2004219)
the Science Foundation of Guangxi Province (No. 0731054)
the Foundation of Innovation Project of Guangxi Graduate Education (No. 2006106020703M32)
