期刊文献+
任意字段
题名或关键词
题名
关键词
文摘
作者
第一作者
机构
刊名
分类号
参考文献
作者简介
基金资助
栏目信息

固相微萃取(SPME)在天然乳脂风味物质分析中的应用研究 被引量：4

下载PDF
导出
摘要 采用固相微萃取吸附富集天然乳脂的挥发性成分。然后用气相色谱-质谱联用分析鉴定,并对3个固相微萃取头进行了比较。天然乳脂的挥发性成分主要是一些酮醛类,酸类和内酯类物质,但不同固相微萃取头对天然乳脂的各挥发性成分的吸附性能有所差别。本试验对CAR/ PDMS、PDMS/DVB、PDMS三种固相微萃取头进行了选择,结合GC—MS分析发现PDMS/DVB对天然乳脂挥发性风味物质的吸附效果最好,能检出21种挥发性物质,其中酮醛类7种,酸类9种,内酯类4种。SPME-GC/MS为乳脂风味物质的研究提供了新的参考方法。
作者 侯园园 王兴国 刘元法
机构地区 江南大学食品学院
出处 《粮油加工》 北大核心 2008年第3期69-71,共3页 Cereals and Oils Processing
关键词 天然乳脂 风味成分 固相微萃取 气相色谱-质谱法
分类号 TS224.4 [轻工技术与工程—粮食、油脂及植物蛋白工程]
  • 相关文献

参考文献9

  • 1李向阳,杨梅,彭宝珠.固相微萃取在生物药物分析中的应用[J].青海医学院学报,2002,23(4):69-71. 被引量：3
  • 2[3]Clark T.J.BunchJ.E.Headspace-solid phase microextraction-gaa chromatography-mass spectrometry analysis of flavorants on tobacco[J].Joumal of AgriculttLral and Food Chemistry,1997,45(3):844.
  • 3刘源,周光宏,徐幸莲.固相微萃取及其在食品分析中的应用[J].食品与发酵工业,2003,29(7):83-87. 被引量：78
  • 4[5]Song J.,Gardner B.D.,Holland J.F.,et al.Rapid analysis of volatile flavor compounds in apple fruit using SPME and gc/time-of-fight mass spectrometry[J].Journal of Agricultural and Food Chemistry,1997,45:1801～1807.
  • 5[6]NgL.k,Hupe M.,Harnois J.,et al.Characterization of commercial vodkas by solid phase microextraction and gas chromatography/mass spectrometry analysis[J].Joumal of Agricultural and Food Chemistry1996,70:380-388.
  • 6[7]Roberts D.D.,PoHien P.,Milo C.Solid-phase microextraction method development for headspaceanalysis of volatile flavor compounds[J].Journal of Agricultural and Food Chemistry,2000,48:2430～2437.
  • 7[8]Coatarini G,Povolo M,Leardi R,et al.Influence of heat treatment on the volatile compounds of milk[J].Agric Food Chem,1997,45:3171～3177.
  • 8[9]Masiliml R.T.SPME-MS-MVA as an electronic nose for the studv of off-flavors in milk[J].Agric Food Cbem,1999,47:648～654.
  • 9[10]Gonzalez-Cordova,Vanejo-Cordoba.Quantitative determination of short-chain free fatty acids in milk using solid-phase mieroextraction and gas chromatography[J].Agric Food Chem,2001,49:4603～4608.

二级参考文献20

  • 1Pawliszyn J. solid phase mieroextraction, wiley, New York, 1998.1
  • 2Arhtur C, Pawliszyn J. solid phase mieroextraction with thermal desorbtion using oused silica optical fibers. Anal chem, 1990, 62:2145
  • 3Zhang Z, Yang M J, Pawliszyn J. solid phase mieroextraction, a solvent -free alternative for sample preparation. Anal chem, 1994, 66:844A
  • 4M. mestres, M. P. Marti, O. Busto et al. simultaneous anaalysis of thiols, sulphides and disulphides in wine aroma by headspace solid phase microextraction - gas chromatography. J chromatography A, 1999,849: 293
  • 5Takeshi Kumazawa, Hiroshi Seno, Xiao- pen Lee et al. Extraction of methylxanthines from human body fluids by solid phase microextraction. Analytica chimica Acta, 1999,387: 53
  • 6Lee XP, Kumazawa Takeshi, Sato Keizo. Detection of tricyclic antidepressants in whole blood by head space solid phase microextraction and capillary chromatography. J chromatogr Sci, 1997,35:302
  • 7T Kumazawa, Sato K, Seno H et al. Extraction of local anaesthetics from human blood by direct immersion - solid phase microextraction, chromatographia, 1996,43:59
  • 8T Kmnazawa, H seno, Watanabe - Suzulki K et al. Determination of phenothiazines in human body fluids by solid phase microextraction and liquid chromatography - tandem mass spectromtry. J mass spectrom,2000,35 (9):1091
  • 9K. Jinno, M. Taniguchi, M. Hayashida. Determination of Benzodizepines in urine by SPMF. - liquid chromatography. J Pharm Biomed Anal, 1998,17:1081
  • 10Ming zhu,Francisco J. Aviles, Eric D. conte et al. Microwave mediated distillation with solid phase microextraction: determination of off- flavors geosmin and methylisoborneol in catfish tissue. J chromatography A, 1999,833:223

共引文献78

同被引文献54

引证文献4

二级引证文献157

粮油加工
2008年 第3期

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部