邻氨基对叔丁基苯酚的合成

Synthesizing Procedure of 2-Amino-4-tert-Butylphenol

对合成邻氨基对叔丁基苯酚的各种路线研究,以及对各种路线所得邻氨基对叔丁基苯酚进行分析应用,确定了以对叔丁基苯酚为原料,用稀硝酸硝化,再进行加氢还原的工艺路线。并在结晶的过程中添加保护剂,得到高收率、高含量并且稳定的白色结晶物。

2 - amino - 4 - tert - butylphenol was synthesized from paratert - butyl phenol with diluted nitric acid and reduction with hydrogen. When protective solute was added 2 - amino - 4 - tert - butylphenol was crystalling.