摘要
以维生素C为催化剂,采用微波辐射无溶剂催化合成环己酮乙二醇缩酮,探索了不同反应条件对产率的影响。实验结果表明,该方法具有反应时间短(3 min)、产率高(78.8%)、无污染等特点。
Cyclohexanone ethylene ketal was synthesized using vitamin C as the catalyst by microwave irradiation solvent-free method. The different conditions affected on yield were investigated. The result showed that the reaction time was short （3 min）, the yields was high（78.8% ） and it had not pollute.
出处
《化工技术与开发》
CAS
2008年第3期20-21,35,共3页
Technology & Development of Chemical Industry
基金
安徽省滁州学院自然科学研究重点项目
批准号:2006kyz004
关键词
微波辐射
无溶剂
维生素C
环己酮乙二醇缩酮
microwave irradiation
solvent-free
vitamin C
cyclohexanone ethylene ketal
