摘要
目的本论文旨在研究常用中药材延胡索的质量控制方法,建立薄层扫描法测定延胡索中延胡索乙素的含量。方法采用双波长反射锯齿扫描,检测波长和参比波长分别为441nm和700nm。结果延胡索乙素在0.2~1.0g范围之间线性良好,平均加样回收率为98.95%,RSD为2.0%。结论上述方法准确,简便,重现性好,可用于延胡索的质量控制。
ObjeetiveA TLCS method was developed for determination of dl - Tetrahyropamative in Rhizoma Corydalis. MethodThe determination was carried out with reflection zigzag scanning at a dual wavelength. The detection wavelength was 410nm and reference wavelength was 700nm. ResultThe linear range was 0.2 - 1.0 ? g. The average recovery was 98:95 % and RSDwas 2.0 %. ConclusionThe method is accurate, simple and can be used for the quality control of Rhizoma Corydalis.
出处
《人参研究》
2008年第1期32-34,共3页
Ginseng Research
关键词
延胡索
延胡索乙素
薄层扫描
质量控制方法
Rhizoma Corydalis
Tetrahyropamative
TLCS
Quality controlled method