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4,4′-二氨基-2,2′-联吡啶的合成及光谱性质

Synthesis and Spectral Properties of 4,4′-Diamino-2,2′-Bipyridine
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摘要 设计出一种简便、有效、安全的4,4′-二氨基-2,2′-联吡啶的超声波合成方法,利用红外光谱、核磁共振氢谱和熔点的测试对产物进行了表征,并测试了产物的紫外-可见吸收光谱和荧光光谱。最终产物的收率有了较大提高。 4, 4＇-diamino-2, 2＇-bipypridine was synthesized in a simple, effective, safe method ultrasonically from 2,2＇-bipypridine. The product was characterized by FT-IR, ^1H NMR spectra and melting point. The UV absorbance spectroscopy and fluorescence was also measured and the yield was increased greatly.
作者 杨茂志 陈秀英 刘延福 郑昌戈
机构地区 江南大学化学与材料工程学院
出处 《光谱实验室》 CAS CSCD 2008年第2期190-194,共5页 Chinese Journal of Spectroscopy Laboratory
关键词 4 4′-二氨基-2 2′-联吡啶 超声波 光谱性质 合成方法 4,4＇-Diamino-2,2＇-Bipypridine,Ultrasonic,Spectroscopy,Synthesis.
分类号 O657.2 [理学—分析化学] O657.33 [理学—分析化学]
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参考文献13

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2008年 第2期

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