摘要
本文采用硫酸二甲酯为主要原料经氯化、氨化合成甲基磺酰胺，产品收率可达６６８％，纯度在９８％以上。
The methane sulfonamide was prepared by using main material dimethyl sulfate which reacts with chlorine,subsquently ammoniating.The yield is 66.8% and the purity is above 98%.The effect of solvent,reaction time and the ratio of material are also discussed.
出处
《农药》
CAS
北大核心
1997年第9期18-19,共2页
Agrochemicals
基金
浙江省教委资助项目
关键词
甲基磺酰胺
合成
氯化
氨化
碘酰胺
methane sulfonamide,synthesis,chlorinating,ammoniating.
