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溶胶-凝胶法制备B_2O_3-SiO_2和RO-B_2O_3-SiO_2系统玻璃薄膜 被引量：3

Preparation of Glass Films of B_2O_3-SiO_2 and RO-BO-SiO System by Sol-Gel Process
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摘要 Glass films of B2O3-SiO2 and RO-B2O3-SiO2 (RO: CaO, MgO, ZnO) system wereprepared by sol-gel process.X-ray diffraction of gels was examided. Ralation oftransmissivity of films to RH,H2O/Si(OC2H5)4(mol), content of B2O3 was measured.Ralation between gelling time and H2O/Si (OC2H5)4(mol) was investigated.IR spectra ofgel and glass of 10B2O3.90SiO2 and 5MgO.10B2O3.80SiO2 system were also measured. Transformation from gel into glass was verified.This work provides a now refereace forpreparation of glass films of boric-silicate by sol-gel process. Glass films of B2O3-SiO2 and RO-B2O3-SiO2 (RO: CaO, MgO, ZnO) system wereprepared by sol-gel process.X-ray diffraction of gels was examided. Ralation oftransmissivity of films to RH,H2O/Si(OC2H5)4(mol), content of B2O3 was measured.Ralation between gelling time and H2O/Si (OC2H5)4(mol) was investigated.IR spectra ofgel and glass of 10B2O3.90SiO2 and 5MgO.10B2O3.80SiO2 system were also measured. Transformation from gel into glass was verified.This work provides a now refereace forpreparation of glass films of boric-silicate by sol-gel process.
作者 刘书君 伍洪标
机构地区 武汉工业大学
出处 《玻璃与搪瓷》 CAS 北大核心 1997年第5期11-16,共6页 Glass & Enamel
关键词 硼硅酸盐玻璃 玻璃薄膜 溶胶凝胶法 玻璃 Sol-gel process Glass films of boric-silicate
分类号 TQ171.718 [化学工程—玻璃工业]
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同被引文献19

  • 1童建喜,张启龙,詹树林.ZnO-B2O3-SiO2溶胶-凝胶制备及表征[J].稀有金属材料与工程,2004,33(z1):129-132. 被引量：2
  • 2张其土,王丽熙,付振晓,许仲梓.铒硼硅酸盐玻璃结构的研究[J].稀土,2006,27(1):19-22. 被引量：10
  • 3Stoch L, Sorda M. Infrared spectroscopy in the investigation of oxide glasses structure[ J]. Mol Struc, 1999,77:511 - 512.
  • 4Sindhu S, sanghi S, Agarwal A, et al. Structural, optical, physical and electrical properties of V2O5 · SrO·B2O3 glasses[J]. Spectrochim Acta A,2005, 64:1196.
  • 5Zhouyun Ren, Chunyan Tao, Hua Yang, et al A novel green emitting phosphor SrAl2B2O7:Tb3 + [J] . Materials Letters,2007 ,61:1654 - 1657.
  • 6郑昌琼,冉均国.新型无机材料[M].北京:科学出版社,2002.
  • 7Guillaume B, Boschini F, Garcia - Cano I, et al. Optimization of BaZrO3 sintering by control of the initial powder size distribution, a factorial design statistical analysis [ J ]. Journal of European Ceramic Society, 2005,25 : 3 593 - 3 604.
  • 8Song K X, Chen X M, Zheng C W. Microwave dielectric characteristics of ceramics in Mg2SiO4 -Zn2SiO4 system [J]. Ceramics International, 2008,34:917 - 920.
  • 9Muralidharan P, Venkateswarlul M, Sotyanarayana N. Sol -gel synthesis, characterization and impedance studies of lithium borosilicate glass[J]. Materials Research Bulletin,2004,39 : 1 753 -1 762.
  • 10Ahmet Kas Bgoz, Takahisa Misono, Yoshimoto Abe. Sol - gel preparation of borosilicates[ J]. Journal of Non - Crystalline Solids, 1999,243 : 168 - 174.

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玻璃与搪瓷
1997年 第5期

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