摘要
采用固相萃取技术对样品进行预处理,建立了优化的合成麝香类化合物的GC-MS分析方法.本方法的分析灵敏度高,可对4种合成麝香类化合物同时分析测定,其最低检测限(LOD)在20—125ng·l-1.该方法对替代物的平均回收率是96.4±8.7%,相对标准偏差(RSD)为9.1%.
The aim of this paper is to develop a simple and convenient method to isolate and concentrate a kind of personal care products（PCPs）——synthetic musks（SMs）. In this paper, solid phase extraction（SPE）was used to extract trace target compounds in water sample.GC-MS was used to determine SMs. The results showed that the instrument was sensitive to the selected SMs. The range of limit of detection（LOD）was as low as 20—125ng·l^-1 . The mean surrogate recoveries were 96.4±8.7%（relative standard deviation（RSD）=9.1%）for fluoranthene d10.
出处
《环境化学》
CAS
CSCD
北大核心
2008年第3期382-384,共3页
Environmental Chemistry
基金
国家自然科学基金(50608050)
上海交通大学青年基金资助项目
