摘要
目的合成柚皮甙、橙皮甙、儿茶素硫酸酯。方法柚皮甙、橙皮甙、儿茶素在冰浴中与浓硫酸反应2 h,用6N NaOH终止反应。衍生物用高效液相色谱(HPLC)-大气压化学电离(APCI)-质谱(MS)联用鉴定。结果和结论有柚皮甙、橙皮甙和儿茶素硫酸酯的生成。
Objective To synthesize and identify the naringin, hesperidin and catechin sulfate. Methods Naringin, hesperidin and catechin were esterified with concentrated sulfuric acid for 2 hours in ice bath, and then terminated by 6N NaOH. Derivatives were identified by HPLC-APCI-MS. Results and Conclusion Naringin, hesperidin and catechin sulfate were produced.
出处
《广东医学院学报》
2008年第2期120-121,134,共3页
Journal of Guangdong Medical College
基金
广东省重点学科基金资助(No:9306)