摘要
用10mLφ(HEl)=0.5的溶液酸化水样,10mL锌氨络盐吸收液,于0.6L/min抽空气30min,溶液吸收硫化物后吸光值稳定,水和废水的测定加标回收率为94.4%~101%,精密度为2.87%~3.27%。改进后的直接显色分光光度法测定水中硫化物,酸化-抽气分离装置简单、操作方便。
The sulfide was determined by improved method of direct spectrophotometry with simple acidification-exhaust separation devices. The method was easily operated by 10 mL φ(HCl) =0.5 acidified sample solution, 0.6 L/min for 30 min air sweeping and absorption was stability. The recoveries of water and wastewater were from 94.4% to 101% , the precisions from 2.87% to 3.27%.
出处
《环境监测管理与技术》
北大核心
2008年第3期64-66,共3页
The Administration and Technique of Environmental Monitoring