摘要
10种未见文献报道的N-[3-(3,4-二甲基-2-吡咯基)-5-巯基-4-均三唑基]-取代芳(氧)酰胺类连杂环化合物通过将5-取代苯基-2-呋喃甲酸及取代苯氧乙酸经酰化后,分别与3-(3,4-二甲基-2-吡咯基)-4-氨基-5-巯基-1,2,4-三唑在乙腈中反应而合成制得.结构经元素分析、IR和1HNMR得到确证.生物活性测试结果表明:大部分目标化合物具有一定的除草活性.
Ten new N-[3-(3,4-dimethyl-1H-pyrrole-2-yl)-5-mercapto-4-triazole]-substituted-aryl(oxy)arn- ides were synthesized by the reaction of 5-(substituted-phenyl)-2-furoyl-chloride or (substituted phenoxy)- acetyl chloride with 3-(3,4-dimethyl-1H-pyrrole-2-yl)-4-amino-5-mercapto-triazole in acetonitrile. The structures of the target compounds were confirmed by ^1H NMR, IR spectra and elemental analysis. The preliminary biological tests show that most of the target compounds have herbicidal activities.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2008年第6期1083-1086,共4页
Chinese Journal of Organic Chemistry
基金
国家自然科学基金(No20672073)
上海市重点学科建设项目(NoT0402)资助项目
关键词
3
4-二甲基吡咯
均三唑
芳(氧)酰胺
除草活性
合成
3,4-dimethyl-1H-pyrrole
1,3,4-triazole
aryl(oxy)amide
herbicidal activity
synthesis