摘要
P-methoxy-N,N-bis(2-cyanoethyl)aniline was synthesized by using p-methoxyaniline,acrylonitrile,AlCl3 and BE.The experimental result had proved that AlCl3 and BE was an excellent catalyst system.The appropriate reactive condition is that AlCl3 was 20%(mol) of p-methoxyaniline,BE was 10%(mol) of p-methoxyaniline,the reaction temperature was 78℃ and the reaction time was 8 hours.The catalyst system had high catalyst efficiency and selectivity together with yield over 94%.
P - methoxy - N, N - bis （2 - cyanoethyl） aniline was synthesized by using p - methoxyaniline, acrylonitrile, AlCl3 and BE. The experimental result had proved that AlCl3 and BE was an excellent catalyst system. The appropriate reactive condition is that AlCl3 was 20% （mol） of p - methoxyaniline, BE was 10% （mol） of p - methoxyaniline, the reaction temperature was 78℃ and the reaction time was 8 hours. The catalyst system had high catalyst efficiency and selectivity together with yield over 94%.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2008年第5期557-560,共4页
Chemical Research and Application
基金
中南林业科技大学引进人才科研基金(030114)资助项目
湖南省科技厅项目(2007FJ4156)
