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流动注射微分光度法测定钛酸钡烧结物中微量钡 被引量:1

The determination of barium in sinter by FIA-double beam of photometric method
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摘要 The mechanism of combination of Flow injection(FIA)and double beam of photometry and testing technique,together with the color reaction condition of 2-(4-bromo-2-carboxy phenylazo)-7-(2,4-dimethyl phenylazo)-1,8-dihydroxynaphthalene-3,6-disulfonic acid reacting with Barium,and the application in the determination of Barium in sinter have been studied.The analyses speed was 130~140 times/h,the Sensitivity was 1.6 times of the ordinary photometric method,the dynamic concentration range of bariumn was 0~1.1μg·mL-1which was in consistent with a Lamber-beer law.The experimental results was satisfactory. The mechanism of combination of Flow injection (FIA)and double beam of photometry and testing technique, together with the color reaction condition of 2-( 4-bromo-2-carboxy phenylazo) -7-( 2,4-dimethyl phenylazo) -1,8-dihydroxynaphthalene-3, 6-disulfonic acid reacting with Barium,and the application in the determination of Barium in sinter have been studied. The analyses speed was 130 - 140 times/h,the Sensitivity was 1.6 times of the ordinary photometric method, the dynamic concentration range of bariumn was 0 - 1.1 μg · mL^-1 which was in consistent with a Lamber-beer law. The experimental results was satisfactory.
出处 《化学研究与应用》 CAS CSCD 北大核心 2008年第5期577-579,共3页 Chemical Research and Application
关键词 流动注射分析 双光束 微量钡 二溴对甲基偶氮溴酸 Flow Injection Analysis micro-barium double beam photometry 2- ( 4-bromo-2-carboxy phenylazo ) -7- ( 2,4-dimethyl phenylazo) -1,8-dihydroxynaphthalene-3, 6-disulfonic acid
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