摘要
目的:对当归芍药散活性部位DSS-A-N-30的化学成分进行研究。方法:用大孔树脂柱色谱制备DSS- A-N-30,用硅胶和反相硅胶柱色谱分离各成分,用MS及NMR技术鉴定结构。结果:从DSS-A-N-30中分离得到了1个新单萜苷。结论:新化合物命名为4″-羟基白芍苷。
Objective： To study the chemical constituents of an active fraction （DSS-A-N-30） from Danggui Shaoyao San. Method： DSS-A-N-30 was prepared by macroporous resin chromatography, the compound was isolated by column chromatography on silica gel and RP C- 18, the structure was elucidated by spectroscopic methods. Result： A new monoterpene glycoside was isolated and identified from DSS-A-N-30. Conclusion： The new monoterpene glycoside was identified as 4＂-hydroxyl-albiflorin.
出处
《中国中药杂志》
CAS
CSCD
北大核心
2008年第12期1413-1415,共3页
China Journal of Chinese Materia Medica
关键词
当归芍药散
化学成分
4″-羟基白芍苷
Danggui Shaoyao San
chemical constituents
4＂-hydroxyl-albiflorin
