期刊文献+

Synthesis, Crystal Structure and Biological Activity of 2-Chloro-N-{2-fluoro-5-[N-(phenylsulfonyl) phenyl-sulfonamido]phenyl}benzamide

Synthesis, Crystal Structure and Biological Activity of 2-Chloro-N-{2-fluoro-5-[N-(phenylsulfonyl) phenyl-sulfonamido]phenyl}benzamide
下载PDF
导出
摘要 2-Chloro-N-{2-fluoro-5-[N-(phenylsulfonyl)phenylsulfonamido]phenyl}benzamide was synthesized and its crystal structure was also determined by X-ray single-crystal diffraction. The title compound(C25H18ClFN2O5S2) belongs to monoclinic, space group P21/n with a=0.7377(3) nm, b=1.2036(5) nm, c=2.6846(11) nm, β=90.895(9)°, V=2.3833(16) nm3, Mr=544.98, Z=4, Dc=1.519 g/cm3, μ=0.385 mm–1, F(000)=1120, R1=0.0632, and wR2=0.1438. Its crystal structure belongs to a novel class that has not been reported yet, and its preliminary herbicidal activity was also tested. Its inhibition rate to seedling growth of barnyard grass reaches 15.1% at 100 μg/mL. 2-Chloro-N-{2-fluoro-5-[N-(phenylsulfonyl)phenylsulfonamido]phenyl}benzamide was synthesized and its crystal structure was also determined by X-ray single-crystal diffraction. The title compound(C25H18ClFN2O5S2) belongs to monoclinic, space group P21/n with a=0.7377(3) nm, b=1.2036(5) nm, c=2.6846(11) nm, β=90.895(9)°, V=2.3833(16) nm3, Mr=544.98, Z=4, Dc=1.519 g/cm3, μ=0.385 mm–1, F(000)=1120, R1=0.0632, and wR2=0.1438. Its crystal structure belongs to a novel class that has not been reported yet, and its preliminary herbicidal activity was also tested. Its inhibition rate to seedling growth of barnyard grass reaches 15.1% at 100 μg/mL.
出处 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2008年第3期295-298,共4页 高等学校化学研究(英文版)
基金 the National Natural Science Foundation of China(Nos.20432010 and 20602021)
关键词 X-ray diffraction Crystal structure SYNTHESIS Biological activity X-ray diffraction Crystal structure Synthesis Biological activity
  • 相关文献

参考文献12

  • 1Shaner D. L., Anderson P. C., Stidham M. A., Plant Physiol., 1984, 76(2), 545
  • 2Pang S. S., Guddat L. W., Duggleby R. G., J. Biol. Chem., 2003, 278(9), 7639
  • 3McCourt J. A., Pang S. S., King-Scott J., et al., Proc. Natl. Acad Sci. USA, 2006, 103(3), 569
  • 4Wang J. G., Xiao Y. J., Li Z. M., et al., Bioorg. Med. Chem., 2007, 15(1), 374
  • 5Wynberg N. A., Leger L. J., Conrad M. L., et al., Can. ,I. Chem., 2005, 83(6/7), 661
  • 6Liu Z. P., Milbum C., Page D., et al., WO, 2005030761, 2005
  • 7Atwal K. S., Ferrara F. N., Ding C. Z., et al., J. Med. Chem., 1996, 39(1), 304
  • 8Leval X. D., Ilies M., Casini A., et al., J. Med Chem, 2004, 47(11), 2796
  • 9Xiao You-jun, Master Dissertation, Chem. Dep. Nankai Univ., 2006
  • 10Sheldrick G. M., SHELXS97 and SHELXL97, University of Gottingen, Gottingen, 1997

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部