摘要
采用TLC跟踪反应,对蔗糖邻苯二甲酸单酯的合成方法进行了系统研究。实验以蔗糖与邻苯二甲酸酐为原料,以氢氧化钾为催化剂,在室温反应3 h,得到了标题化合物,产率62%。
TLC was used to track the reactions related with the synthesis of phthalic acid sucrose monoester. Using sucrose and phthalic anhydride as reagents and potassium hydrate as the catalyst at room temperature in 3 h, the phthalic acid sucrose monoester was obtained and the yield of product was equal to 62%.
出处
《化学试剂》
CAS
CSCD
北大核心
2008年第7期531-532,共2页
Chemical Reagents