摘要
Ethyl cellulose is coated on 3-aminopropyl silica gel,with optical resolution ability as chiral stationary phase(CSPs) for high-performance liquid chromatography is evaluated with a flow rate of 0.5 mL/min at 30℃.All the test solutes are detected at 254nm.Among 15 resolved racemates,6 chiral compounds could be separated in the normal phase condition,1 chiral compound in the reversed phase and 2 chiral compounds in acetonitrile condition.The results show that the chiral stationary phase possess good selectivity.
Ethyl cellulose is coated on 3 - aminopropyl silica gel, with optical resolution ability as chiral stationary phase（CSPs） for high - performance liquid chromatography is evaluated with a flow rate of 0.5 mL/min at 30℃. All the test solutes are detected at 254nm. Among 15 resolved racemates,6 chiral compounds could be separated in the normal phase condition,1 chiral compound in the reversed phase and 2 chiral compounds in acetonitrile condition. The results show that the chiral stationary phase possess good selectivity.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2008年第7期935-938,共4页
Chemical Research and Application
基金
云南省自然科学基金重点项目(2005E0006Z)
