2,6-二乙基苯胺基乙基丙基醚的合成

The synthesis of 2,6-Diethyl-N-(2-propoxyethyl)aniline

以2,6-二乙基苯胺与氯乙基丙基醚为原料,合成了2,6-二乙基苯胺基乙基丙基醚,对反应条件进行优化,确定了最佳工艺条件为:反应时间10h,反应温度170℃,原料配比n(2,6-二乙基苯胺):n(氯乙基丙基醚)=3:1,碱浓度为40%。在此条件下反应,摩尔收率可达到85.6%。

2,6-Diethyl-N-（2-propoxyethyl）aniline can be synthesized by 2,6-diethylaniline and 2-ehloro-1ethoxypropane. According to the analysis of experimental results, optimum conditions obtained were as follows： reaction time 10h, temperature 170℃, 3：1 material molar ratio of 2,6-diethylaniline to 2-ehloro-l-ethoxypropane. Under these conditions, the product molar yield was 85.6%.