摘要
溴代金刚烷和醇在Ag2S04作用下,方便地合成了一系列的金刚烷单醚(收率70.6%-96.0%)和金刚烷二醚(收率35.0%-64.0%),其结构经^1HNMR和”CNMR表征。
A series of adamantyl ethers were synthesized by the reaction of bromoadamantanes with alcohols in the presence of Ag2SO4. The yield of adamantyl monoethers and adamantyl diethers were 70.6% - 96.0% and 35.0% - 64.0%, respectively. The structures Were confirmed by ^1H NMR and ^13 C NMR.
出处
《合成化学》
CAS
CSCD
2008年第4期467-469,471,共4页
Chinese Journal of Synthetic Chemistry
基金
浙江省科技计划资助项目(2006C31028)
关键词
金刚烷
醚
合成
adamantane
ether
synthesis