摘要
目的:提高护肝片的质量标准。方法:采用薄层色谱法对护肝片中五味子、猪胆粉、茵陈进行鉴别;采用高效液相色谱法测定五味子乙素和绿原酸的含量。结果:薄层色谱法可检出五味子、猪胆粉、茵陈,斑点清晰,阴性对照无干扰。高效液相色谱法测定五味子乙素、绿原酸含量。平均回收率分别为99.9%,RSD为1.1%,99.7%,RSD为1.4%(n=6)。结论:方法简单,可以用于护肝片质量控制。
Objective: To improve the quality standard for Hugan tablets. Method: Fructus schisanderae Chinensis, Pulvis fellis Suis, Herba artemisiae Scopariae were identified by TLC. The contents of γ-Schinzandrin and chlorogenic acid were determined by HPLC. Result: Fructus schisanderae Chinensis, Pulvis fellis Suis, Herba artemisiae Scopariae could be identified by TLC, the spots were clear the negative control with non-interfere. The average recoveries( n =6) of γ-Schinzandrin and chlorogenic acid were 99.9% and 99.7% with RSD 1.1% and 1.4% ( n = 6), respectively. Conelusion: The method is simple, it can be used for the quality control of Hugan tablets.
出处
《中国药师》
CAS
2008年第8期950-952,共3页
China Pharmacist