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离子色谱法测定草甘膦异丙胺盐的含量 被引量:2

Determination of Glyphosate-isopropylammonium by Ion Chromatography
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摘要 采用离子色谱法测定了草甘膦异丙胺盐的含量。用AS–11离子色谱柱(含AG–11离子色谱保护柱)和电导检测器、外标法对草甘膦异丙胺盐进行定性、定量分析,方法的相对标准偏差为1.60%~1.74%,标准添加回收率为98.3%~101.5%。该方法方便快速,结果准确可靠。 Determination of glyphosate-isopropylammonium by ion chromatography (IC) was described. The Glyphosate-isopropylammonium was quantitatively and qualitatively determined by IC with a conductivity detector, a AG-11 and AS-11 column, and an external standard. Relative standard deviation was 1.60% to 1.74%, and average recoveries between 98.3% and 101.5% were obtained for spiked samples. The method is simple, rapid, accurate and reliable.
作者 武中平 高巍
出处 《现代农药》 CAS 2008年第4期31-32,35,共3页 MODERN AGROCHEMICALS
基金 江苏省质量技术监督局2007年资助科研项目(KJ073501)
关键词 草甘膦异丙胺盐 离子色谱法 测定 glyphosate-isopropylammonium ion chromatography determination
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  • 1中国农业科学院植物保护研究所.农药分析[M].北京:化学工业出版社,1990.259-260.
  • 2[2]Young J C, Kahn S V. Analytical teehniques of glyphosate residue analysis [J]. J Agrie Food Chem,1977,25:918-922.
  • 3[3]Dibyendu N Roy, Samir K. Konar development of an analytical method for the determination of glyphosate residues in soil by nitrogen-selective gas chromatography [J]. J Agric Food Chem,1989,37:441-443.
  • 4GB 12686-1990.草甘膦原药[S],1990.
  • 5H. Anson Moye,et al.Asimplified High- performance Liquid Chromatographic Residue Procedure for the Determination of Glyphosate Herbicide and (Aminomethyl) phosphonic Acidin Fruits and Vegetables Employing Postcolumn Fluorgenic Labeling[].Journal of Agricultural and Food Chemistry.1983
  • 6Cynthia L. Deyrup,et al.Simultaneous Esterification and Acylation of Pesticides for Analysis by Gas Chromatography.1. Derivatization of Glyphosate and Alcohols-Perfluorinated Anhydrides[].Journal of Agricultural and Food Chemistry.1995
  • 7James N. Seiber,et al.Analysis of Glyphosate Residues in Kiwi Fruit and Asparagus Using High-Performance Liquid Chromatography of Derivatized Glyphosate as a Cleanup Step[].Journal of Agricultural and Food Chemistry.1984
  • 8Kelvin,P.Spann &Phillip.A. Hargreaves, The Determination of Glyphosate in Soils with Moderate to High Clay content[].Pesticide Science.1994
  • 9Moye, H. A,Boning, A. J. Analytical Letters . 1979
  • 10周淑光.草甘膦及其分解产物的检验研究[J].刑事技术,1996,21(6):13-15. 被引量:1

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