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IC法同时分析6种重金属离子最佳测定条件

Study on the optimal conditions for determination of heavy metals synchronously by ion chromatogram
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摘要 使用双功能柱离子色谱-柱后衍生-PeakNet软件-紫外可见检测法,探讨了满足Ⅳ水质要求的微量可溶态重金属离子Pb2+、Cu2+、Cd2+、Co2+、Zn2+和Ni2+共存的最佳测定条件。讨论了此条件下,山西区域内高硬度水质中Ca2+、Mg2+离子对上述6种离子同时测定的影响。 In this paper, the optimal conditions on the simultaneous determination of trace heavy metals being dissolved (Pb^2+ ,Cu^2+ Cd^2+ ,Co^2+ Zn^2+ and Ni^2+ ) at vg/L levels were studied, which satisfied IV water quality demand. The metal ions were separated by ion chromatography on a mixed bead ion exchange column and detected by post-colunm reaction and UV/visible spectro-photomet- tic detection and Peak Net software. Furthermore, it was discussed that the Ca^2+ and Mg^2+ in the high hardness water from Shanxi interfered with separation and quantitative analysis of the metals for the proposed method.
出处 《山西化工》 2008年第4期33-35,61,共4页 Shanxi Chemical Industry
关键词 离子色谱法 柱后衍生 重金属离子 高硬度水 ion chromatogram post column derivatization heavy metal ions high hardness water
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参考文献13

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