摘要
本文分析了NMR外标参比积分法中影响测定精度的各种因素,通过实例说明了饱和效应、偏置效应和旋转边带对测定精度的影响程度,并指出了消除各种误差的有效方法。
A quantitative NMR method by using an external reference has been developed. Various factors which affect its precision, such as saturation effect, offset effect and the effect of rotation sidebands,are discussed in detail.The method is suitable for determining common inorganic ions.
出处
《分析化学》
SCIE
EI
CAS
CSCD
北大核心
1989年第2期136-138,共3页
Chinese Journal of Analytical Chemistry
关键词
NMR
核磁共振
定量法
外标
参比
NMR
Quantitative method
Saturation effect
Offset effect
Sidebands