摘要
本文将毛细管气相色谱与Nicolet 5sxc富里叶变换红外光谱联机检测应用于含挥发油的中成药的分析研究。对红灵散中的冰片、麝香酮分别进行了定性定量分析。将红灵散的苯提取液作GC/FTIR定性分析,用气相色谱内标校正因子法测定冰片、麝香酮的含量,其中冰片的加样回收率平均值为100.1％,相对标准偏差为2.0％,麝香酮的加样回收率平均值为97.80％,相对标准偏差为3.5％。
Chinese herbal preparations Hong Lingsan including volatile oil was studied by capillary GC/FTIR. Bornyl, isobornyl and muskone were determined qualitatively and quantitatively by GC internal standard method. The average recovery of 100.1％ and RSD of 2.0％ for bornyl, and average recovery of 97.80％ and RSD of 3.5％ for muskone are obtained.
出处
《分析化学》
SCIE
EI
CAS
CSCD
北大核心
1989年第3期231-235,共5页
Chinese Journal of Analytical Chemistry
关键词
中成药
红灵散
红外光谱
冰片
Capillary GC/FTIR
Hong Lin gsan
Bornyl
Muskone
