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Preparation and Structural Investigation of CuCl_2 Graphite Intercalation Compounds 被引量：4

Preparation and Structural Investigation of CuCl_2 Graphite Intercalation Compounds
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摘要 Superfine graphite powder was prepared by ball-milling exfoliated graphite containing anhydrous CuCl2 in planetary ball milling systems. Nano-scale CuCl2 graphite intercalation compounds were synthesized by heating a mixture of anhydrous CuCl2 and graphite nanosheets. Scanning electron microscopy, energy-dispersive X-ray spectroscopy and high-resolution transmission electron microscopy were performed to characterize the microstructures of stage-1 nano-scale CuCl2 graphite intercalation compounds. The structure and components of the domain wall and core in the nano-scale CuCl2 graphite intercalation compounds are described. The results show that the content of CuCl2 in the mixture plays a crucial role in the size of the nano-scale CuCl2 graphite intercalation compound. Superfine graphite powder was prepared by ball-milling exfoliated graphite containing anhydrous CuCl2 in planetary ball milling systems. Nano-scale CuCl2 graphite intercalation compounds were synthesized by heating a mixture of anhydrous CuCl2 and graphite nanosheets. Scanning electron microscopy, energy-dispersive X-ray spectroscopy and high-resolution transmission electron microscopy were performed to characterize the microstructures of stage-1 nano-scale CuCl2 graphite intercalation compounds. The structure and components of the domain wall and core in the nano-scale CuCl2 graphite intercalation compounds are described. The results show that the content of CuCl2 in the mixture plays a crucial role in the size of the nano-scale CuCl2 graphite intercalation compound.
作者 BIN Xiaopei CHEN Jiazang CAO Hong MA Enbao WANG Xuehua YUAN Jizhu
机构地区 School of Resource and Environmental Engineering School of Materials Science and Engineering State Key Laboratory of Coal Conversion
出处 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2008年第5期1056-1060,共5页 地质学报（英文版）
基金 the National Natural Science Fund(50774071） ；the Natural Science Foundation of Hubei Province(2004ABA090）.
关键词 NANO-SCALE graphite intercalation compounds DOMAIN structure nano-scale, graphite intercalation compounds, domain, structure
分类号 X591 [环境科学与工程—环境工程]
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参考文献7

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共引文献3

同被引文献30

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Acta Geologica Sinica(English Edition)
2008年 第5期

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